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Alpha Lipoic acid

   
 

Certificate of Analysis

Alpha Lipoic Acid (Thioctic acid)

Molecular formula: C8H14O2S2

Molecular weight:  206.33                             Structural formular:

 


Batch No.  020814                                MFG Date:   8/12/2002

                                                EXP Date:    8/12/2004

Quantity:   100  kgs                              Report Date:  8/20/2002  

Test Items                   Specifications                     Test Results

Appearance               Yellowish crystalline powder              Conforms

Identification              Lead Acetate test and UV, IR:Positive       Conforms

Melting Point(BP)          60-62                                       62

Solubility(IN NaOH)        Clear and pale yellow                    Conforms

Residue on ignition         0.10%                               0.10%

Heavy Metals              10 ppm                              10ppm

Chloride                  0.07%                               0.07%

Loss on Drying            0.50%                                 0.16%

Assay(by HPLC)          99.00%                                99.52%

Specific optical rotation       -1--+1                               Conforms

Related substance (by HPLC) 

Single impurity             0.20%                              0.15%

6,8-Epitrithloctic acid        0.30%                              0.26%

Total impurities             0.50%                              0.43%

Polymere                  0.50%                              0.50%

Residual solvents(GC)

Toluene                    5 ppm                              5 ppm

Cyclohexane                0.20%                              0.11%

Ethylacetate                5 ppm                               5 ppm

Microbiology              

Total aerobic counts         1000CFU/g                      100CFU/g

Mould                     100CFU/g                      Not detectable

Ecol                    Not detectable                        Not detectable

Salamonellas             Not detectable                        Not detectable

 

   
       
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     Best regards from SHENZHEN , China

                                                       Mr. JEFFERY TSUI

   
       
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